African Journal of
Pharmacy and Pharmacology

  • Abbreviation: Afr. J. Pharm. Pharmacol.
  • Language: English
  • ISSN: 1996-0816
  • DOI: 10.5897/AJPP
  • Start Year: 2007
  • Published Articles: 2288

Full Length Research Paper

Volatiles in the Lysimachia clethroides Duby by head space solid phase microextraction coupled with gas chromatography-mass spectrometry (HS-SPME-GC-MS)

Jin-Feng Wei1,2,3, Zhen-hua Yin2 and Fu-De Shang1*
1College of Life Science, Henan University, Kaifeng 475004, China. 2Institute of Chinese Materia Medica, Henan University, Kaifeng 475004, China. 3Minsheng College, Henan University, Kaifeng 475004, China.
Email: [email protected]

  •  Accepted: 13 August 2012
  •  Published: 05 September 2012

Abstract

We studied for the first time, the volatile compounds in the Lysimachia clethroide Duby by using head space solid phase microextraction (HS-SPME) coupled with gas chromatography-mass spectrometry (GC-MS). The results showed that 14 compounds were identified from the stem of L. clethroides, 13 compounds were identified from the leaves, and 16 compounds from the flowers. 8 compounds were mutual components, accounting for 92.99, 94.59 and 90.32% of the identified components in stem, leaves and flowers, respectively. Limonene was the main compound in the three parts, and the contents were up to 52.59, 54.57 and 44.98%, respectively. These showed that the volatiles had not much difference in the three parts; maybe the three parts have the same medicinal effect, and could provide certain theoretical basis for further development and utilization.

 

Key words: Lysimachia clethroides Duby, solid phase microextraction, volatiles.