Journal of
Medicinal Plants Research

  • Abbreviation: J. Med. Plants Res.
  • Language: English
  • ISSN: 1996-0875
  • DOI: 10.5897/JMPR
  • Start Year: 2007
  • Published Articles: 3835

Full Length Research Paper

Preparative purification of coniferyl ferulate from Angelica sinensis oil by high performance centrifugal partition chromatography

Yue Yu, Qing-Wen Zhang* and Shao-Ping Li
Institute of Chinese Medical Sciences, University of Macau, Taipa, Macau SAR, China.
Email: [email protected]

  •  Accepted: 18 November 2010
  •  Published: 04 January 2011

Abstract

A high performance centrifugal partition chromatography (HPCPC) method was successfully developed to purify coniferyl ferulate (CF) from the extracts of commercialAngelica sinensis oil by using n-hexane-ethyl acetate-ethanol-water (5:5:5:5, v/v) as the two-phase solvent system. The upper and lower phases of this system were used as stationary and mobile phases, respectively. The purity of coniferyl ferulate was over 98% as determined by high-performance liquid chromatography (HPLC). The structure of coniferyl ferulate was identified by MS, 1H NMR and 13C NMR.

 

Key words: Angelica sinensis, coniferyl ferulate, high performance centrifugal partition chromatography, solvent extraction.

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This article is published under the terms of the Creative Commons Attribution License 4.0

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